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Electroanalytical Methods in Pharmaceutical Analysis and Their Validation |
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Sibel A. Ozkan |
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$99.75 |
October 2011 |
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Illustrated: |
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Contents
Preface
1. Drugs
Versus Chemicals: Similarities and Differences
Arzu
Onay-Besikci and Sibel A. Ozkan
1.1. Peripheral Nervous System Drugs
1.2. Central Nervous System Drugs
1.3. Cardiovascular and Renal Drugs
1.4. Endocrine Drugs
1.5. Chemotherapeutic Drugs
1.6. Anti-inflammatory, Antiallergic, and
Immunoregulatory Drugs
1.7. Development of Drugs
References
2. Electroanalytical
Chemistry
Sibel
A. Ozkan
References
3. Experimental
Considerations
Sibel
A. Ozkan
3.1. Reference Electrode
3.2. Auxiliary (Counter) Electrode
3.3. Electroanalytical Conditions
References
4. Working
Electrodes
Sibel
A. Ozkan
4.1. Mercury Electrodes
4.1.1. Dropping Mercury Electrodes
4.1.2. Hanging Mercury Drop Electrodes
4.1.3. Static Mercury Drop Electrodes
4.1.4. Mercury Film Electrodes
4.2. Solid Electrodes
4.2.1. Noble Metal Electrodes
4.2.2. Carbon Electrodes
4.2.2.1. Graphite Electrodes
4.2.2.2. Fullerene and Carbon Nanotube Electrodes
4.2.2.3. Carbon Fibers
4.2.2.4. Screen-Printed Electrodes
4.2.2.5. Carbon Paste Electrodes
4.2.2.6. Glassy Carbon Electrodes
4.2.2.7. Diamond Electrodes
4.2.2.8. Chemically Modified Electrodes
References
5. Classical
Potential Sweep Methods in Pharmaceutical
Analysis
Sibel
A. Ozkan
5.1. Applications of LSV in Pharmaceutical Analysis
5.2. Applications of CV in Pharmaceutical Analysis
5.3. Summary
References
6. Controlled
Potential and Pulsed Voltammetric
Techniques in Pharmaceutical
Analysis
Bengi
Uslu and Sibel A. Ozkan
6.1. Polarography
6.2. Pulse Polarography/Voltammetry
6.2.1. Normal Pulse Voltammetry/Polarography
6.2.2. AC Voltammetry/ Polarography
6.2.3. Differential Pulse Polarography/Voltammetry (DPV)
6.2.4. Square-Wave Voltammetry
6.2.5. Staircase Voltammetry
References
7. Stripping
Techniques in Pharmaceutical Analysis
Sibel
A. Ozkan
7.1. Anodic Stripping Voltammetry
7.2. Cathodic Stripping Voltammetry
7.3. Adsorptive Stripping Voltammetry
7.4. Potentiometric Stripping Analysis
7.5. Abrasive Stripping Voltammetry
References
8. Practical
Applications in Pharmaceutical and
Biomedical Chemistry
Sibel
Suzen and Sibel A. Ozkan
8.1. Electrochemistry in Drug Development and
Analysis
8.1.1. Benzimidazoles
8.1.2. Indoles
8.1.3. Catechols
8.1.4. Benzofuran
8.1.5. Quinones
8.1.6. Antibiotics
8.1.7. Steroids
8.1.8. Other Drug Molecules
8.2. Metabolite Determination Using Electrochemical
Methods
8.3. Oxidative Stress
8.4. Electrochemical Therapy
References
9. Method
Validation
Sibel
A. Ozkan
9.1. Validation
Processes of Electroanalytical Methods
9.2. Validation
Characteristics of Electroanalytical Methods
9.2.1. Specificity and Selectivity
9.2.2. Linearity
9.2.3. Range
9.2.4. Sensitivity
9.2.5. Limit of Detection
9.2.6. Limit of Quantitation
9.2.7. Accuracy
9.2.8. Precision
9.2.9. Robustness
9.2.10. Ruggedness
9.2.11. Stability
References
Abbreviations and
Symbols
Index
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